and O
and O.M. the hydrochlorides of these alkaloids (1C10) were prepared by reported method [10]. As shown in Physique 2, common LC-MS chromatograms for a standard solution mixture under UV (260 nm) and MS detections by electrospray ionization (ESI) MS under the positive mode demonstrated good baseline separation for all those peaks. Each peak was observed at the following retention time Mouse monoclonal to EhpB1 and quasimolecular ion peak ([M + H]+) (296), 2 (39.5 min, 282), 3 (29.7 min, 282), 4 (21.3 min, 268), 5 (13.9 min, 312), 6 (16.9 min, 314), 7 (15.9 min, 300), 8 (9.9 min, 300), 9 (8.3 min, 286), and 10 (18.8 min, 286)). These peaks were unambiguously assigned by comparison of their retention times with those of authentic specimens [2]. Open in Nandrolone propionate…